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5679-00-5
- Product Name:Minocycline EP Impurity D
- Molecular Formula:C21H23N3O7
- Purity:99%
- Molecular Weight:429.43
Product Details;
CasNo: 5679-00-5
Molecular Formula: C21H23N3O7
Factory Sells Best Quality Minocycline EP Impurity D 5679-00-5 with GMP standards
- Molecular Formula:C21H23N3O7
- Molecular Weight:429.43
- Melting Point:>213?C (dec.)
- Boiling Point:817.4±65.0 °C(Predicted)
- PKA:4.50±1.00(Predicted)
- PSA:187.41000
- Density:1.65±0.1 g/cm3(Predicted)
- LogP:0.98430
5679-00-5 Relevant articles
Preparation method of 7-amino-6-demethylation-6-deoxy tetracycline and minocycline hydrochloride
-
Paragraph 0324; 0325; 0330; 0331; 0334; 0335, (2021/04/14)
The invention relates to a preparation m...
Synthesis method of minocycline hydrochloride
-
Paragraph 0319; 0323-0325, (2021/06/21)
The invention relates to a synthesis met...
Preparation method of 7-aminominocyclin
-
Paragraph 0026-0028, (2019/10/02)
The invention discloses a preparation me...
Substituted Tetracycline Compounds
-
Page/Page column 114, (2010/12/29)
The present invention pertains, at least...
5679-00-5 Process route
-
-
7-amino-6-demethyltetracycline

-
-
5679-00-5
7-amino-6-desmethyl-6-deoxytetracycline
Conditions | Yield |
---|---|
With
sulfuric acid; 5% rhodium-on-charcoal; hydrogen;
In
methanol;
at 40 ℃;
for 8h;
under 18751.9 Torr;
Temperature;
Pressure;
Autoclave;
|
88.1% |
-
-
808-26-4,2696-12-0,15964-02-0,39105-46-9
sancycline

-
-
5679-00-5
7-amino-6-desmethyl-6-deoxytetracycline
Conditions | Yield |
---|---|
sancycline;
With
dibenzyl azodicarboxylate; trifluoroacetic acid;
at 5 - 10 ℃;
for 7h;
With
hydrogen;
5%-palladium/activated carbon;
In
methanol;
for 3h;
under 2068.65 Torr;
|
5679-00-5 Upstream products
-
[4S-(4a,12aα)]-7-nitro-3,10,12,12a-tetrahydroxy-1,11-dioxo-1,4,4a,5,5a,6,11,12a octahydro-naphthacene-2-carboxylic acid amide
-
sancycline
-
dibenzyl azodicarboxylate
-
demeclocycline hydrochloride
5679-00-5 Downstream products
-
sancycline
-
minocycline Hydrochloride
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